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1-Heptanamine → N"-heptylguanidine hydrate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Heptanamine | HCID 8127 | — |
| 反応物 | HCID 178483237 | HCID 178483237 | — |
| 生成物 | N"-heptylguanidine hydrate | HCID 86736194 | 132% |
反応手順
A mixture of heptylamine (1.15 g) and N-cyano-N'-[2-[[[5-(dimethylamino)methyl-2-furanyl]methyl]thio]ethyl]carbamimidothioic acid (3.12 g) was heated on an oil bath for 12 hr at 100°. The product was chromatographed (silica/methanol) to give N-cyano-N'-[2-[[[5-dimethylamino)methyl-2-furanyl]methyl]thio]ethyl]-N"-heptylguanidine hydrate (2.31g) Rf 0.49. Analysis Found: C, 56.99; H, 8.32; N, 17.53. C19H33N5OS.H2O requires: C, 57.43; H, 8.81; N, 17.63%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04128658 |
| 出典データセット | uspto-grants-1978_12 |
| ORD ID | ord-c04d4b0fcdf24f159071070d9a7a63eb |
| 出典メモ | uspto-grants-1978_12 |