化工社化工社 化学情報印刷レポート · 研究参考用
Dimethyladipate → Disodium adipate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dimethyladipate | HCID 12329 | — |
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 溶媒 | Acetonitrile | HCID 6342 | — |
| 生成物 | Disodium adipate | HCID 24073 | — |
反応手順
17.4 g. (0.1 mole) of dimethyl adipate were dissolved in 100 mls. of acetonitrile and heated to 70° C. 8.2 g. (0.2 mole) of 97% pure sodium hydroxide were added to the reaction mixture as a fine powder (50 mesh). The reaction mixture was stirred at reflux temperature for 18 hours. The resulting solution was filtered hot and the solids were air dried to yield disodium adipate as the reaction product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04129520 |
| 出典データセット | uspto-grants-1978_12 |
| ORD ID | ord-af3c1eef92454c249d5f397014b710cf |
| 出典メモ | uspto-grants-1978_12 |