化工社化工社 化学情報印刷レポート · 研究参考用
Diazomethane → Methyl 3,5-Dibromobenzoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Diazomethane | HCID 9550 | — |
| 反応物 | Benzoic acid, 3,5-dibromo- | HCID 12063 | — |
| 溶媒 | Diethyl Ether | HCID 3283 | — |
| 生成物 | Methyl 3,5-Dibromobenzoate | HCID 621923 | — |
反応手順
To a solution of 3,5-dibromobenzoic acid (1 eq.) in ether was added dropwise a solution of diazomethane in ether until gas evolution had ceased. The reaction was stirred for 20 min and concentrated in vacuo to afford the title compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08076359B2 |
| 出典データセット | uspto-grants-2011_12 |
| ORD ID | ord-c9c0b78b58ea4da49f17993ef5b5aaae |
| 出典メモ | uspto-grants-2011_12 |