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Ethanol → Sodium 8-aminonaphthalene-1,3,5-trisulfonate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethanol | HCID 702 | — |
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | 8-Aminonaphthalene-1,3,5-trisulfonic acid | HCID 87355 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Sodium 8-aminonaphthalene-1,3,5-trisulfonate | HCID 10343683 | — |
反応手順
To a mixture of 26.6 g of 8-amino-1,3,5-naphthalenetrisulfonic acid in 25 ml of water is added 12 ml of 5N sodium hydroxide. This solution is added to 125 ml of ethanol and stirred for 30 minutes. The resulting solid is recovered by filtration, washed with 50 ml of 80% ethanol followed by ethanol and ether and dried at 110° C. giving 8-amino-1,3,5-naphthalenetrisulfonic acid trisodium salt.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04129591 |
| 出典データセット | uspto-grants-1978_12 |
| ORD ID | ord-63dad3697ee74cb4b39486bd094061c4 |
| 出典メモ | uspto-grants-1978_12 |