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2-Acetylamino-4-aminotoluene → 4-[2-(3,5-Dimethoxy-phenylamino)-oxazol-5-yl]-benzonitrile
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Acetylamino-4-aminotoluene | HCID 79492 | — |
| 反応物 | N-(3,5-dimethoxyphenyl)acetamide | HCID 702039 | — |
| 反応物 | 4-[2-(5-Amino-2-methyl-phenylamino)-oxazol-5-yl]-benzonitrile | HCID 17757346 | — |
| 生成物 | 4-[2-(3,5-Dimethoxy-phenylamino)-oxazol-5-yl]-benzonitrile | HCID 24871996 | 85% |
反応手順
The same procedure outlined above in the preparation of 4-[2-(5-Amino-2-methyl-phenylamino)-oxazol-5-yl]-benzonitrile was used. However N-(3,5-dimethoxyphenyl)-acetamide was used instead N-(5-amino-2-methyl-phenyl)-acetamide. Yield=85%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08080669B2 |
| 出典データセット | uspto-grants-2011_12 |
| ORD ID | ord-97f4d324d02c4d80b084fbac4c70776d |
| 出典メモ | uspto-grants-2011_12 |