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4-[2-(5-Amino-2-methyl-phenylamino)-oxazol-5-yl]-benzonitrile → 4-(2-(5-Amino-2-methylphenylamino)-4-chlorooxazol-5-yl)-2,6-dimethylbenzonitrile
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-[2-(5-Amino-2-methyl-phenylamino)-oxazol-5-yl]-benzonitrile | HCID 17757346 | — |
| 反応物 | 4-(2-Chlorooxazol-5-yl)benzonitrile | HCID 68443558 | — |
| 反応物 | 4-(2,4-Dichlorooxazol-5-yl)-2,6-dimethylbenzonitrile | HCID 68443575 | — |
| 生成物 | 4-(2-(5-Amino-2-methylphenylamino)-4-chlorooxazol-5-yl)-2,6-dimethylbenzonitrile | HCID 24872115 | 74% |
反応手順
The same procedure outlined above in the preparation of 4-[2-(5-Amino-2-methyl-phenylamino)-oxazol-5-yl]-benzonitrile was used. However 4-(2,4-dichlorooxazol-5-yl)-2,6-dimethylbenzonitrile was used instead 4-(2-Chloro-oxazol-5-yl)-benzonitrile. Yield=74%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08080669B2 |
| 出典データセット | uspto-grants-2011_12 |
| ORD ID | ord-4ec7fc8e5945464bac93baab64c5e2b7 |
| 出典メモ | uspto-grants-2011_12 |