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Pyridine → Butyl 7-(tert-butylperoxy)-3,7-dimethyloctyl carbonate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Pyridine | HCID 1049 | — |
| 反応物 | Butyl chloroformate | HCID 61140 | — |
| 反応物 | 3,7-Dimethyl-7-(t-butylperoxy)octyl alcohol | HCID 53664183 | — |
| 溶媒 | Diethyl Ether | HCID 3283 | — |
| 生成物 | Butyl 7-(tert-butylperoxy)-3,7-dimethyloctyl carbonate | HCID 23346617 | — |
反応手順
To a solution of 7.9 g (0.03 mole) of 3,7-dimethyl-7(t-butylperoxy)octyl alcohol and 2.4 g (0.03 mole) of pyridine in diethyl ether cooled at 10°±1° C was added a solution of 4.09 (0.03 mole) of n-butyl chloroformate in diethyl ether. The reaction temperature was maintained at 15°±1° C during the addition.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04129700 |
| 出典データセット | uspto-grants-1978_12 |
| ORD ID | ord-22cf3ce5ef674b899ba6e662b054e132 |
| 出典メモ | uspto-grants-1978_12 |