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Diethyl Ether → 7-Chloro-1-methyllepidinium iodide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Diethyl Ether | HCID 3283 | — |
| 反応物 | Methyl iodide | HCID 6328 | — |
| 反応物 | 7-Chloro-4-methylquinoline | HCID 170437 | — |
| 溶媒 | Acetonitrile | HCID 6342 | — |
| 生成物 | 7-Chloro-1-methyllepidinium iodide | HCID 22016371 | — |
反応手順
A portion of the 7-chlorolepidine (80 mg) prepared as above was methylated by heating with CH3I (0.5 ml) in CH3CN (1 ml) at reflux for two hours. The mixture was treated with diethyl ether, followed by centrifugation, to give a yellow powder.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07083982B2 |
| 出典データセット | uspto-grants-2006_08 |
| ORD ID | ord-6a873647e2b44ce99055068705e47796 |
| 出典メモ | uspto-grants-2006_08 |