Hydrochloric Acid → HCID 53870487、化合物

反応式

Cl[CH2:2][CH2:3][O:4][C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][C:6]=1[CH:11]=[CH:12][C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1.[CH3:19][NH:20][CH3:21].Cl>>[CH3:19][N:20]([CH3:21])[CH2:2][CH2:3][O:4][C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][C:6]=1[CH:11]=[CH:12][C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1

参加物

反応物 3

HCID 313Hydrochloric Acid

HCID 674Dimethylamine

HCID 537953612-(beta-Chloro-ethoxy)-stilbene

生成物 1

HCID 53870487HCID 53870487、化合物

実験手順

2-(β-Dimethylamino-ethoxy)-stilbene was prepared from 2-(β-chloro-ethoxy)-stilbene and dimethylamine, and the free base was converted into its hydrochloride, yielding 45% of theory of the compound of the formula ##STR14## which had a melting point of 199° C.