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2,6-Dichloroaniline → 3-Benzoyl-2',6'-dichloroacrylanilide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2,6-Dichloroaniline | HCID 11846 | — |
| 反応物 | Pentafluoroaniline | HCID 13040 | — |
| 反応物 | Phosphorus pentachloride | HCID 24819 | — |
| 反応物 | 2-Benzoylprop-2-enoic acid | HCID 15839051 | — |
| 反応物 | 3-(Benzoyl)pentafluoroacrylanilide | HCID 85847495 | — |
| 生成物 | 3-Benzoyl-2',6'-dichloroacrylanilide | HCID 85847494 | — |
反応手順
The following additional compounds are prepared by employing PCl5 reagent in accordance with the method of the above Example 6. An analogous quantity of the appropriate benzoylacrylic acid or a substituted benzoylacrylic acid is employed in the manner of the benzoylacrylic acid of Example 5. Likewise, an analogous quantity of the appropriately substituted aniline is employed in the manner of the 2,6-dichloroaniline. Thus, to prepare 3-(benzoyl)pentafluoroacrylanilide, an analogous amount of benzoylacrylic acid is employed and there is used an analogous quantity of pentafluoroaniline in place of the 2,6-dichloroaniline.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04130661 |
| 出典データセット | uspto-grants-1978_12 |
| ORD ID | ord-3d7c09b7671b429ca9133e350ed4823e |
| 出典メモ | uspto-grants-1978_12 |