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HRID 66153作成日:2026年10月27日

2,6-Dichloroaniline → 3-Benzoyl-2',6'-dichloroacrylanilide

https://huagongshe.com/reaction/66153

反応式

関与物質

役割名称HCID仕込み量
反応物2,6-DichloroanilineHCID 11846—
反応物PentafluoroanilineHCID 13040—
反応物Phosphorus pentachlorideHCID 24819—
反応物2-Benzoylprop-2-enoic acidHCID 15839051—
反応物3-(Benzoyl)pentafluoroacrylanilideHCID 85847495—
生成物3-Benzoyl-2',6'-dichloroacrylanilideHCID 85847494—

反応手順

The following additional compounds are prepared by employing PCl5 reagent in accordance with the method of the above Example 6. An analogous quantity of the appropriate benzoylacrylic acid or a substituted benzoylacrylic acid is employed in the manner of the benzoylacrylic acid of Example 5. Likewise, an analogous quantity of the appropriately substituted aniline is employed in the manner of the 2,6-dichloroaniline. Thus, to prepare 3-(benzoyl)pentafluoroacrylanilide, an analogous amount of benzoylacrylic acid is employed and there is used an analogous quantity of pentafluoroaniline in place of the 2,6-dichloroaniline.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04130661
出典データセットuspto-grants-1978_12
ORD IDord-3d7c09b7671b429ca9133e350ed4823e
出典メモuspto-grants-1978_12