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4-Oxobutanoic acid → 1-Piperidinium
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Oxobutanoic acid | HCID 1112 | — |
| 反応物 | Piperidine | HCID 8082 | — |
| 溶媒 | Benzene | HCID 241 | — |
| 生成物 | 1-Piperidinium | HCID 637969 | — |
| 生成物 | 4-Oxobutanoate | HCID 9543238 | — |
反応手順
100 Mg. of 4-(8-methoxy-6,11-dihydrodibenzo-[b.e.]-thiepin-11-one-3-yl)-4-oxobutyric acid in 10 ml. of benzene is treated with 60 mg. of piperidine. The solution obtained is allowed to stand for one hour and the crystalline material which forms is filtered, washed with ether and air dried to yield piperidinium 4-(8-methoxy-6,11-dihydrodibenzo-[b.e.]-thiepin-11-one-3-yl)-4-oxobutyrate.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04130654 |
| 出典データセット | uspto-grants-1978_12 |
| ORD ID | ord-95cdf6991778486985518cab3455bb88 |
| 出典メモ | uspto-grants-1978_12 |