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4-Chlorobutanoic acid → Tri-n-butyl(carboxypropyl)phosphonium Chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Chlorobutanoic acid | HCID 12300 | — |
| 反応物 | Tributylphosphine | HCID 13831 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | Tri-n-butyl(carboxypropyl)phosphonium Chloride | HCID 85918976 | — |
反応手順
Tri-n-butyl phosphine (0.1 mole) and 4-chlorobutyric acid (0.1 mole) were refluxed in toluene for 4 hours. Evaporation of the solvent from the reaction mixture left a viscous liquid whose infrared spectrum and elemental analysis corresponded to a compound of the formula
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04131633 |
| 出典データセット | uspto-grants-1978_12 |
| ORD ID | ord-c0497a2fdd6846519d384910679bcf61 |
| 出典メモ | uspto-grants-1978_12 |