化工社化工社 化学情報印刷レポート · 研究参考用
Thionyl Chloride → 3-Phenyl-3-(4-nitrophenyl)propenoyl chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 反応物 | 3-(4-Nitrophenyl)-3-phenylprop-2-enoic acid | HCID 53427600 | — |
| 溶媒 | Benzene | HCID 241 | — |
| 生成物 | 3-Phenyl-3-(4-nitrophenyl)propenoyl chloride | HCID 54529932 | — |
反応手順
A mixture of 22 g. of 3-phenyl-3-(4-nitrophenyl)propenoic acid, 11.7 g. of thionyl chloride and 150 ml. of benzene was heated under reflux for 1 hour. The solvent was removed by evaporation in vacuo, and the residual solid was recrystallized from carbon tetrachloride. This afforded 20 g. of the title compound, m.p. 117°-120° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04342781 |
| 出典データセット | uspto-grants-1982_08 |
| ORD ID | ord-c9dc609ad93844f48364bf8bb6e0a502 |
| 出典メモ | uspto-grants-1982_08 |