化工社化工社 化学情報印刷レポート · 研究参考用
Methylparaben → 4-(1,1,2,3,3,3-Hexafluoropropyloxy)-benzoic acid methyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methylparaben | HCID 7456 | — |
| 反応物 | Hexafluoropropylene | HCID 8302 | — |
| 反応物 | Potassium Hydroxide | HCID 14797 | — |
| 溶媒 | Acetone | HCID 180 | — |
| 生成物 | 4-(1,1,2,3,3,3-Hexafluoropropyloxy)-benzoic acid methyl ester | HCID 54298519 | — |
反応手順
456 g (3 moles) of 4-hydroxybenzoic acid methyl ester, 30 g of 85% potassium hydroxide, and 1 l of acetone were placed in an autoclave. An amount of 562.5 g (3.75 moles) of hexafluoropropylene was introduced under pressure.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04342825 |
| 出典データセット | uspto-grants-1982_08 |
| ORD ID | ord-8cdc38c5c0b74bd7b36fdf8f5926c27e |
| 出典メモ | uspto-grants-1982_08 |