化工社化工社 化学情報印刷レポート · 研究参考用
Pentaerythritol → Pentaerythritol Tetrakis(2,4-dimethoxybenzoate)
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Pentaerythritol | HCID 8285 | — |
| 反応物 | 2,4-Dimethoxybenzoyl chloride | HCID 2734719 | — |
| 生成物 | Pentaerythritol Tetrakis(2,4-dimethoxybenzoate) | HCID 20530744 | 78% |
反応手順
Using the procedure of Eample I, 2,4-dimethoxybenzoyl chloride was allowed to react with pentaerythritol in the molar ratio of 4:1. The reaction gave a 78% yield of white crystalline product having a melting point of 125°-126.5° C. and the infrared spectrum was a consistent with the expected tetraester with no hydroxyl band and an ester carbonyl band at 5.85μ (s).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04342875 |
| 出典データセット | uspto-grants-1982_08 |
| ORD ID | ord-42dfaebc9cba4c71a19c8c1f54691fa8 |
| 出典メモ | uspto-grants-1982_08 |