関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Ethylene Glycol | HCID 174 | — |
| 反応物 | 2-Butoxyethanol | HCID 8133 | — |
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | Sodium 2-butoxyethanolate | HCID 23671990 | — |
反応手順
Into a 1 liter three-necked flask, equipped as described in Example 1, 590 g of 3-oxaheptan-1-ol (i.e., the butyl monoether of ethylene glycol) are introduced. 40 g of sodium hydroxide in pellet form are added and the mixture is heated to 120° C. Sodium 3-oxaheptan-1-olate and water are formed, with the latter being removed by distillation.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04343745 |
|---|
| 出典データセット | uspto-grants-1982_08 |
|---|
| ORD ID | ord-020eaacd7a70428bb6e9f7e9503c1602 |
|---|
| 出典メモ | uspto-grants-1982_08 |
|---|
