関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Hydrochloric Acid | HCID 313 | — |
| 反応物 | Tris(2-chloroethyl)amine hydrochloride | HCID 61220 | — |
| 反応物 | Sodium 2-butoxyethanolate | HCID 23671990 | — |
| 生成物 | 2-(2-butoxyethoxy)-N,N-bis[2-(2-butoxyethoxy)ethyl]ethanamine | HCID 4102023 | — |
反応手順
When all of the water of the reaction has been eliminated, 55 g of tris(2-chloroethyl)amine hydrochloride are introduced. The mixture is heated at 130° C. for 5 hours, then cooled. Excess sodium alcoholate is then neutralized with a 10% aqueous solution of hydrochloric acid. The 3-oxaheptan-1-ol is removed by distillation and the sodium chloride is removed by filtration. The desired product, tris(3,6-dioxadecyl)amine, is distilled (192° C. under 0.1 mmHg).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 特許番号 | US04343745 |
|---|
| 出典データセット | uspto-grants-1982_08 |
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| ORD ID | ord-5377dfd8cac4454ea970e3feec082f2e |
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| 出典メモ | uspto-grants-1982_08 |
|---|
