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HRID 67045作成日:2026年10月24日

Benzeneacetic acid, 4-chloro-alpha-(1-methylethyl)- → 2-(4-Chlorophenyl)-3-methylbutanoyl chloride

https://huagongshe.com/ja/reaction/67045

反応式

関与物質

役割名称HCID仕込み量
反応物Benzeneacetic acid, 4-chloro-alpha-(1-methylethyl)-HCID 16197—
反応物Thionyl ChlorideHCID 24386—
生成物2-(4-Chlorophenyl)-3-methylbutanoyl chlorideHCID 4178001—

反応手順

10 g of the product of Step D were added to a mixture of 50 ml of petroleum ether (b.p.=35°-70° C.) and 20 ml of thionyl chloride and the mixture was refluxed for 4 hours and was then cooled. The mixture was evaporated to dryness to obtain 10.8 g of D 2-isopropyl-2-p-chlorophenyl acetyl chloride.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04344895
出典データセットuspto-grants-1982_08
ORD IDord-55d226453b9140adbbf9185143dcf950
出典メモuspto-grants-1982_08