Diazomethane → HCID 20528716、化合物

HRID 67175ノート

反応式

HRID 67175 の反応式
[C:1]([C:4]1[CH:14]=[CH:13][CH:12]=[C:6]2[C:7]([NH:9][C:10](=[O:11])[C:5]=12)=[O:8])([OH:3])=[O:2].[N+](=[CH2:17])=[N-]>CCOCC>[CH3:17][O:2][C:1]([C:4]1[CH:14]=[CH:13][CH:12]=[C:6]2[C:7]([NH:9][C:10](=[O:11])[C:5]=12)=[O:8])=[O:3]

参加物

4

反応物 2

HCID 9550DiazomethaneHCID 205447191,3-dioxo-2,3-dihydro-1H-isoindole-4-carboxylic acid

生成物 1

HCID 20528716HCID 20528716、化合物

試薬・触媒・溶媒 1

HCID 3283Diethyl Ether溶媒2 回

実験手順

To a suspension of 3-carboxyphthalimide (10 g) in ether (50 ml), a solution of diazomethane in ether was added slowly until a faint yellow colouration persisted. Excess of diazomethane was destroyed with acetic acid and the reaction mixture was evaporated to yield the desired compound.

後処理

  1. customExcess of diazomethane was destroyed with acetic acid
  2. customthe reaction mixture was evaporated

出典と根拠

ORDレコード
ord-76be70ed1a3f490eb78799c7bb42183a
出典データセット
uspto-grants-1982_08
特許番号
US04345071

反応ノート

読み込み中…