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cis-4-(3-Chlorophenyl)-but-3-enylamine → 4-(3-Chlorophenyl)butan-1-amine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | cis-4-(3-Chlorophenyl)-but-3-enylamine | HCID 58679830 | — |
| 反応物 | HCID 178418361 | HCID 178418361 | — |
| 触媒 | Platinum dioxide monohydrate | HCID 11139377 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | 4-(3-Chlorophenyl)butan-1-amine | HCID 10655071 | 74.2% |
反応手順
A solution of cis-4-(3-chlorophenyl)-but-3-enylamine (1.2 g) in 20 mL methanol was added to platinum(IV) oxide monohydrate (0.12 g). The mixture was stirred under 1 atm of hydrogen for 16 h. The mixture was filtered through celite, and the methanol was removed in vacuo to yield 0.9 g of 4-(3-chlorophenyl)-butylamine.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07084154B2 |
| 出典データセット | uspto-grants-2006_08 |
| ORD ID | ord-6eda0c359052479e89b251fa31711b9d |
| 出典メモ | uspto-grants-2006_08 |