化工社化工社 化学情報印刷レポート · 研究参考用
N-(2-Hydroxyethyl)ethylenediamine → 4-Behenoyloxyethyl-2,3,6,7-tetrahydro-1,4-diazocin-5-one
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | N-(2-Hydroxyethyl)ethylenediamine | HCID 8112 | — |
| 反応物 | Docosanoic Acid | HCID 8215 | — |
| 反応物 | Methyl 4-oxobutyrate | HCID 83779 | — |
| 生成物 | 4-Behenoyloxyethyl-2,3,6,7-tetrahydro-1,4-diazocin-5-one | HCID 54163854 | — |
反応手順
Into an apparatus similar to that in Example 1, were charged 104.2 g (1 mole) of N-hydroxyethylethylenediamine and 116.1 g (1 mole) of methyl 3-formylpropionate. At 130° C., 18 g of water and 32 g of methanol were distilled off. After adding 340.5 g (1 mole) of behenic acid, esterification was carried out at 210° to 220° C. to obtain 4-behenoyloxyethyl-2,3,6,7-tetrahydro-1,4-diazocin-5-one.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04346087 |
| 出典データセット | uspto-grants-1982_08 |
| ORD ID | ord-df1a55e079f2490d9fdb51575a250049 |
| 出典メモ | uspto-grants-1982_08 |