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Acetone → HCID 178482500、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Acetone | HCID 180 | — |
| 反応物 | 3-(Trifluoromethyl)benzoyl chloride | HCID 75257 | — |
| 反応物 | N-Methylhydrazinecarbothioamide | HCID 2723853 | — |
| 溶媒 | Pyridine | HCID 1049 | — |
| 生成物 | HCID 178482500 | HCID 178482500 | — |
反応手順
A 42 g. portion of 4-methylthiosemicarbazide was reacted with 200 ml. of acetone, and then with 32 g. of pyridine and 83.6 g. of 3-trifluoromethylbenzoyl chloride. The mixture was worked-up as described in Example 1 to obtain 77.5 g. of the desired product, m.p. 111°-115°, after recrystallization from nitromethane.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04346225 |
| 出典データセット | uspto-grants-1982_08 |
| ORD ID | ord-bd0437614152434bb4e32c1135ec93de |
| 出典メモ | uspto-grants-1982_08 |