関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Pyridine | HCID 1049 | — |
| 反応物 | Diketene | HCID 12661 | — |
| 反応物 | Aminoethyl methacrylate hydrochloride | HCID 75495 | — |
| 溶媒 | Dimethylformamide | HCID 6228 | — |
| 生成物 | 2-[(3-Oxobutanoyl)amino]ethyl 2-methylprop-2-enoate | HCID 22023972 | 60% |
反応手順
Pyridine (16 g, 0.2 mole) was added dropwise at 0° C. to a solution of 2-aminoethyl methacrylate hydrochloride (33 g, 0.2 mole) and diketene (16.8 g, 0.2 mole) in N,N-dimethylformamide (600 ml). After the addition, the solution was stirred at 20° C. for 20 hours. The solvent was then removed at low vacuum. The residue was dissolved in chloroform (1200 ml), washed with water (twice with 200 ml), dried over anhydrous magnesium sulfate and filtered. Excess solvent was then removed. Distillation of the residue gave acetoacetamidoethyl methacrylate (b.p.=113°-132° C./5μ) at a yield of 60%.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 特許番号 | US04346231 |
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| 出典データセット | uspto-grants-1982_08 |
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| ORD ID | ord-c1b6394eb0dd4f16b8b3e809a5b361ac |
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| 出典メモ | uspto-grants-1982_08 |
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