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Sarcosine → 1-Methyl-3-n-nonyl hydantoin
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Sarcosine | HCID 1088 | — |
| 反応物 | Hydantoin | HCID 10006 | — |
| 反応物 | Sodium Hydroxide | HCID 14798 | — |
| 反応物 | capric N-chloramide | HCID 19040089 | — |
| 溶媒 | Water | HCID 962 | — |
| 溶媒 | tert-Butanol | HCID 6386 | — |
| 生成物 | 1-Methyl-3-n-nonyl hydantoin | HCID 70549405 | 90% |
反応手順
In accordance with the procedure described in Example 6, 41 g (0.2 mol) capric N-chloramide were reacted with sarcosine, sodium hydroxide in a mixture of tertiary butanol and water and then processed. The hydantoin remained in the aqueous solution was an oil, that was extracted with ether. The ether was removed by distillation to yield 43 g (90% yield) 1-methyl-3-n-nonyl hydantoin of the formula ##STR10## having the following analysis:
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04346233 |
| 出典データセット | uspto-grants-1982_08 |
| ORD ID | ord-37b99b25d34c4e0887d8172c6d4f7e0f |
| 出典メモ | uspto-grants-1982_08 |