Isopropanol → N-methyl-N-(2,3,4,5,-6-pentahydroxy-n-hexyl)-N'-n-undecyl urea

関与物質

反応手順

A mixture containing 7 g (30 mmol) of lauric N-chloramide dissolved in 200 ml of isopropanol, was reacted with a solution containing 5.85 g (30 mmol) of N-methyl-D-glucamine in 150 ml of isopropanol, 40 ml of water and 1.2 g (30 mmol) of sodium hydroxide at 50° C. for a period of 1 hour. The reaction mixture was processed in accordance with the procedures described in Example 12 to yield 7.38 g (63% yield) of N-methyl-N-(2,3,4,5,-6-pentahydroxy-n-hexyl)-N'-n-undecyl urea of the formula ##STR13## having a melting point of 109° C. and the following analysis:

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