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HRID 6806作成日:2026年10月23日

N-ethyl-3-methyl-6-nitroquinolin-2-amine → n2-Ethyl-3-methylquinoline-2.6-diamine

https://huagongshe.com/ja/reaction/6806

反応式

関与物質

役割名称HCID仕込み量
反応物N-ethyl-3-methyl-6-nitroquinolin-2-amineHCID 22018880—
触媒Platinum oxide (PtO)HCID 82844—
溶媒MethanolHCID 887—
生成物n2-Ethyl-3-methylquinoline-2.6-diamineHCID 85837566—

反応手順

The product (0.8 g) of Step B and platinum oxide on carbon (˜80 mg) was suspended in methanol. The resulting mixture was hydrogenated at 50 PSI for 1 h. The reaction mixture was filtered through filter aid and the solvent removed under vacuum to afford the product, which was used without further purification.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US07084156B2
出典データセットuspto-grants-2006_08
ORD IDord-bc1ae466ad6d421a8c6e6bc08d31abd8
出典メモuspto-grants-2006_08