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N-ethyl-3-methyl-6-nitroquinolin-2-amine → n2-Ethyl-3-methylquinoline-2.6-diamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | N-ethyl-3-methyl-6-nitroquinolin-2-amine | HCID 22018880 | — |
| 触媒 | Platinum oxide (PtO) | HCID 82844 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | n2-Ethyl-3-methylquinoline-2.6-diamine | HCID 85837566 | — |
反応手順
The product (0.8 g) of Step B and platinum oxide on carbon (˜80 mg) was suspended in methanol. The resulting mixture was hydrogenated at 50 PSI for 1 h. The reaction mixture was filtered through filter aid and the solvent removed under vacuum to afford the product, which was used without further purification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07084156B2 |
| 出典データセット | uspto-grants-2006_08 |
| ORD ID | ord-bc1ae466ad6d421a8c6e6bc08d31abd8 |
| 出典メモ | uspto-grants-2006_08 |