Benzene, 1-bromo-3-iodo- → 3-(3-Bromophenyl)phenanthrene
反応式
BrC1C=CC([C:8]2[CH:21]=[CH:20][C:19]3[C:18]4[C:13](=[CH:14][CH:15]=[CH:16][CH:17]=4)[CH:12]=[CH:11][C:10]=3[CH:9]=2)=CC=1.C1(B(O)O)C2C=CC3C(=CC=CC=3)C=2C=CC=1.[Br:39][C:40]1[CH:41]=[C:42](I)[CH:43]=[CH:44][CH:45]=1>>[Br:39][C:40]1[CH:45]=[C:44]([C:10]2[CH:11]=[CH:12][C:21]3[CH:20]=[CH:19][C:18]4[C:17]([C:8]=3[CH:9]=2)=[CH:16][CH:15]=[CH:14][CH:13]=4)[CH:43]=[CH:42][CH:41]=1参加物
4
実験手順
Synthesis was performed in the same manner as in the synthesis of 2-(4-bromophenyl)phenanthrene except that: phenanthrene-1-boronic acid was used instead of phenanthrene-2-boronic acid; and 3-bromoiodobenzene was used instead of 4-bromoiodobenzene.
後処理
- customSynthesis
出典と根拠
- ORDレコード
- ord-c7b9cc7e0b7641138220821dcffe5a89
- 出典データセット
- uspto-grants-2014_09
- 特許番号
- US08822041B2
反応ノート
読み込み中…