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4-Methoxy-2-methylbenzoic acid → (S)-7-[4-(4-methoxy-2-methyl-benzoylamino)-phenyl]-2,7-diaza-spiro[4.4]nonane-2-carboxylic acid tert-butyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Methoxy-2-methylbenzoic acid | HCID 597216 | — |
| 反応物 | (S)-7-(4-amino-phenyl)-2,7-diaza-spiro[4.4]nonane-2-carboxylic acid tert-butyl ester | HCID 68994472 | — |
| 生成物 | (S)-7-[4-(4-methoxy-2-methyl-benzoylamino)-phenyl]-2,7-diaza-spiro[4.4]nonane-2-carboxylic acid tert-butyl ester | HCID 68990294 | — |
反応手順
According to Method P, (S)-7-(4-amino-phenyl)-2,7-diaza-spiro[4.4]nonane-2-carboxylic acid tert-butyl ester was reacted with 4-methoxy-2-methyl-benzoic acid. In this way the product was obtained with molecular weight 465.60 (C27H35N3O4); MS (ESI): 466 (M+H+).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08822495B2 |
| 出典データセット | uspto-grants-2014_09 |
| ORD ID | ord-4411a7611f2e413ca00db0c0a4c00637 |
| 出典メモ | uspto-grants-2014_09 |