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6-Aminobenzothiazole → 4-Nitrophenyl benzo[d]thiazol-6-ylcarbamate hydrochloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 6-Aminobenzothiazole | HCID 68288 | — |
| 反応物 | 4-Nitrophenyl chloroformate | HCID 82129 | — |
| 溶媒 | Dichloromethane | HCID 6344 | — |
| 生成物 | 4-Nitrophenyl benzo[d]thiazol-6-ylcarbamate hydrochloride | HCID 66797303 | 81% |
反応手順
6-Aminobenzothiazole (100 mg, 0.666 mmol) and p-nitrophenyl chloroformate (148 mg, 0.733 mmol) were stirred at rt in CH2Cl2 (5 mL) overnight. The resulting solid was collected by filtration, yielding 183 mg (81%) of the title compound. LC-MS: RT=8.17 min, [M+H]+=316.0.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08822472B2 |
| 出典データセット | uspto-grants-2014_09 |
| ORD ID | ord-5b5b00a8a2234c6e86c3e37c49c0c5b4 |
| 出典メモ | uspto-grants-2014_09 |