化工社化工社 化学情報印刷レポート · 研究参考用
p-Bromophenethylamine → 4'-(2-Aminoethyl)-3-biphenylcarboxamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | p-Bromophenethylamine | HCID 533915 | — |
| 反応物 | (3-Carbamoylphenyl)boronic acid | HCID 2737814 | — |
| 反応物 | Toluene ethanol | HCID 21863594 | — |
| 溶媒 | 1,2-Dimethoxyethane | HCID 8071 | — |
| 生成物 | 4'-(2-Aminoethyl)-3-biphenylcarboxamide | HCID 58276405 | — |
反応手順
The title compound was prepared from 3-(aminocarbonyl)-phenyl boronic acid and 4-bromophenethylamine according to the procedure described for intermediate I-VII-1 with the exceptions that 4:1 PhMe/EtOH was sued as organic solvent (instead of DME) and the chromatographic purification step was omitted. LC/MS (method E) 0.53 min; m/z 241 (M+H).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08822518B2 |
| 出典データセット | uspto-grants-2014_09 |
| ORD ID | ord-d3081091b1fe44fa8a47eb45f5cae40c |
| 出典メモ | uspto-grants-2014_09 |