化工社化工社 化学情報印刷レポート · 研究参考用
3-Aminoquinuclidine → N-[[[1-Azabicyclo[2.2.2]octan-3-yl]amino]carbonyl]-2-methoxybenzamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-Aminoquinuclidine | HCID 123238 | — |
| 反応物 | 2-Methoxybenzoyl isocyanate | HCID 14119328 | — |
| 生成物 | N-[[[1-Azabicyclo[2.2.2]octan-3-yl]amino]carbonyl]-2-methoxybenzamide | HCID 15616380 | 105.5% |
反応手順
This compound was prepared by the procedure of example 1, using 3-aminoquinuclidine (0.63 g, 5 mmol) and 2-methoxybenzoyl isocyanate (1.0 g, 5 mmol), giving crude title product (1.6 g) which was purified as its 1:1 fumarate mp 187°-188° C. (0.79 g)
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04983600 |
| 出典データセット | uspto-grants-1991_01 |
| ORD ID | ord-56d6b96aa0874275869dd2bbaad40d3b |
| 出典メモ | uspto-grants-1991_01 |