関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | 1,1-Dichlorosilacyclobutane | HCID 75373 | — |
| 反応物 | 2-Trimethylsilylacetate | HCID 22558220 | — |
| 生成物 | 1,1-Diacetoxysilacyclobutane | HCID 15065919 | — |
反応手順
To 30.0 g trimethylsilylacetate was added 16.0 g 1,1-dichlorosilacyclobutane. The reactants were stirred for one hour at 25° C. and fractional distillation performed on the reaction mixture. The title compound was isolated as a clear, colorless fluid. The yield was 14.6 g (81.4%). The structure of the product was confirmed by mass spectroscopy and nuclear magnetic resonance spectroscopy (NMR).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04985565 |
|---|
| 出典データセット | uspto-grants-1991_01 |
|---|
| ORD ID | ord-bee8c52996154db1b1910529339899a1 |
|---|
| 出典メモ | uspto-grants-1991_01 |
|---|
