Water → HCID 49856399、化合物
反応式
[N:1]1([C:6]2[CH:7]=[C:8]3[C:13](=[CH:14][CH:15]=2)[N:12]=[C:11]([C:16]2[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=2)[N:10]=[CH:9]3)[CH:5]=[CH:4][N:3]=[CH:2]1.[OH2:22]>CO>[OH2:22].[N:1]1([C:6]2[CH:7]=[C:8]3[C:13](=[CH:14][CH:15]=2)[N:12]=[C:11]([C:16]2[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=2)[N:10]=[CH:9]3)[CH:5]=[CH:4][N:3]=[CH:2]1参加物
4
実験手順
50 mg of 6-(1H-imidazol-1-yl)-2-phenylquinazoline are suspended in 2 mL of methanol, the suspension is heated at reflux for a few minutes, and then filtered and left to evaporate slowly at room temperature, at rest. The crystals obtained are analysed. XRPD: Form C. TGA: weight loss: 6.32% (theoretical value for C17H12N4.H2O: 6.2%), TGA-IR in agreement with the IR spectrum of H2O for the released vapours.
後処理
- temperaturethe suspension is heated