反応式
[N:1]1[CH:6]=[CH:5][CH:4]=[CH:3][C:2]=1[C:7]([O:9]CC)=O.[NH2:12][NH2:13].C(OCC)C>C(O)C>[N:1]1[CH:6]=[CH:5][CH:4]=[CH:3][C:2]=1[C:7]([NH:12][NH2:13])=[O:9]参加物
5
反応条件
- 温度
- 80 °C
実験手順
A mixture of ethyl pyridin-2-carboxylate (90 gm) and hydrazine (60 gm) in ethanol (400 ml) was stirred at 80° C. over a period of 4 h. Solvent was evaporated and to provide a crude mass. The mass was stirred with diethyl ether and the suspension was filtered and the wet cake washed with small quantity of ethanol (50 ml) to provide title compound in 76 gm quantity (93%) as a white solid.
後処理
- customSolvent was evaporated
- customto provide a crude mass
- filtrationthe suspension was filtered
- washthe wet cake washed with small quantity of ethanol (50 ml)
出典と根拠
- ORDレコード
- ord-d650448a01824a70a2ecd839870847ed
- 出典データセット
- uspto-grants-2015_11
- 特許番号
- US09175031B2
関連ノート
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