関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Propyl Acetate | HCID 7997 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | Ethanol n-propyl acetate | HCID 22155088 | — |
反応手順
The dried high DS starch hexanoate described above (Ex. 12, 71.3 g), ethanol (65.2 g), and n-propyl acetate (65.2 g) were charged to a 500 mL round bottom flask, equipped with condenser, overhead stirrer, nitrogen blanket, thermocouple and heating mantle. The mixture was heated to 60° C. for about 1 hr. to form a transparent, low viscosity solution at 30 wt % solids in 50/50 ethanol/n-propyl acetate.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 特許番号 | US09175179B2 |
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| 出典データセット | uspto-grants-2015_11 |
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| ORD ID | ord-ba198b69b5fb4b6aaa592aab49863e33 |
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| 出典メモ | uspto-grants-2015_11 |
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