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Phosphoric Acid → Codeinone 14-Hydroxycodeinone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Phosphoric Acid | HCID 1004 | — |
| 反応物 | (4R,4aS,12bS)-4a-hydroxy-9-methoxy-3-methyl-2,4,7a,13-tetrahydro-1H-4,12-methanobenzofuro[3,2-e]isoquinolin-7-one | HCID 5359420 | — |
| 反応物 | Codeinone | HCID 5459910 | — |
| 生成物 | Codeinone 14-Hydroxycodeinone | HCID 131726012 | — |
反応手順
25±1 mg of both codeinone and 14-hydroxycodeinone reference materials were weighed and transferred into a 100-mL volumetric flask, diluted to volume and dissolved with ˜0.85% phosphoric acid solution II.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08822687B2 |
| 出典データセット | uspto-grants-2014_09 |
| ORD ID | ord-035af55de6134fabbd797eb93ee1d4e8 |
| 出典メモ | uspto-grants-2014_09 |