化工社化工社 化学情報印刷レポート · 研究参考用
Oxalyl chloride → Dimethyl-1,3-oxazole-5-carbonyl chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Oxalyl chloride | HCID 65578 | — |
| 反応物 | Dimethyl-1,3-oxazole-5-carboxylic acid | HCID 1132979 | — |
| 溶媒 | Dichloromethane | HCID 6344 | — |
| 生成物 | Dimethyl-1,3-oxazole-5-carbonyl chloride | HCID 12336332 | — |
反応手順
To a stirring solution of 2,4-dimethyl-oxazole-5-carboxylic acid (30 mg) in DCM (2.0 mL), oxalyl chloride (3.0 eq) was added at room temperature. The reaction mixture was stirred for 30 minutes. Solvents were evaporated and dried under vacuo to afford 2,4-dimethyl-oxazole-5-carbonyl chloride.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09175003B2 |
| 出典データセット | uspto-grants-2015_11 |
| ORD ID | ord-051aa11aea3d49acb73551ed03209563 |
| 出典メモ | uspto-grants-2015_11 |