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3-Chloro-4-isopropoxybenzaldehyde → 3-Chloro-4-(propan-2-yloxy)benzoic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-Chloro-4-isopropoxybenzaldehyde | HCID 4339889 | — |
| 反応物 | 3-Chloro-4-ethoxybenzaldehyde | HCID 4770035 | — |
| 生成物 | 3-Chloro-4-(propan-2-yloxy)benzoic acid | HCID 22597728 | 98% |
反応手順
When the 3-chloro-4-isopropoxybenzaldehyde was substituted for 3-chloro-4-ethoxybenzaldehyde in Example 49, Step A the identical process afforded the title compound in 98% yield, as a colourless solid. 1H-NMR (CDCl3) 1.4 (d, 6H, J=5.1 Hz); 4.67 (m, 1H); 6.95 (m, 1H); 7.96 (m, 1H); 8.10 (m, 1H).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09181182B2 |
| 出典データセット | uspto-grants-2015_11 |
| ORD ID | ord-b0058cda07e94abfa0f83bf66ffc69d5 |
| 出典メモ | uspto-grants-2015_11 |