反応式
[CH3:1][S:2][C:3]1[CH:8]=[CH:7][C:6]([CH2:9][CH2:10][C:11](O)=O)=[CH:5][CH:4]=1.C1CCC(N=C=NC2CCCCC2)CC1.[N:29]1[C:33]2[CH:34]=[CH:35][C:36]([C:38]([NH:40][NH2:41])=O)=[CH:37][C:32]=2[NH:31][CH:30]=1.COC1C=CC(P2(SP(C3C=CC(OC)=CC=3)(=S)S2)=[S:51])=CC=1>>[CH3:1][S:2][C:3]1[CH:8]=[CH:7][C:6]([CH2:9][CH2:10][C:11]2[S:51][C:38]([C:36]3[CH:35]=[CH:34][C:33]4[NH:29][CH:30]=[N:31][C:32]=4[CH:37]=3)=[N:40][N:41]=2)=[CH:5][CH:4]=1参加物
5
実験手順
The compound was synthesized starting from 3-(4-methylthiophenyl)propionic acid (197 mg; 1 mmol), DCC (206 mg; 1 mmol), benzimidazol-5-carbohydrazide (176 mg; 1 mmol) and Lawesson's reagent (606 mg; 1.5 mmol) as described in method 2; yield: 0.029 mg (8.2%);
後処理
- customThe compound was synthesized
出典と根拠
- ORDレコード
- ord-930049d94c9443b3abc9a831d25f7b65
- 出典データセット
- uspto-grants-2015_11
- 特許番号
- US09181233B2
関連ノート
読み込み中…