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Triethylamine → HCID 178497575、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Triethylamine | HCID 8471 | — |
| 反応物 | 3-Chlorophenethylamine | HCID 139381 | — |
| 反応物 | HCID 178497571 | HCID 178497571 | — |
| 反応物 | HCID 178497576 | HCID 178497576 | — |
| 溶媒 | Acetonitrile | HCID 6342 | — |
| 生成物 | HCID 178497575 | HCID 178497575 | — |
反応手順
2-{4-[2-(3-Chloro-phenyl)-ethylamino]-2-oxo-1,2-dihydro-pyridin-3-yl}-3H-benzoimidazole-4-carboxylic acid methyl ester was synthesized from 2-(4-chloro-2-oxo-1,2-dihydro-pyridin-3-yl)-3H-benzoimidazole-4-carboxylic acid methyl ester, 2-(3-Chloro-phenyl)-ethylamine, triethylamine, and ACN using a similar procedure as 2-[4-((S)-2-hydroxy-2-phenyl-ethylamino)-2-oxo-1,2-dihydro-pyridin-3-yl]-3H-benzoimidazole-4-carboxylic acid methyl ester yielding 2-{4-[2-(3-chloro-phenyl)-ethylamino]-2-oxo-1,2-dihydro-pyridin-3-yl}-3H-benzoimidazole-4-carboxylic acid methyl ester.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09181218B2 |
| 出典データセット | uspto-grants-2015_11 |
| ORD ID | ord-42b59bd04fd34de59b3cac88e53c5d69 |
| 出典メモ | uspto-grants-2015_11 |