化工社化工社 化学情報印刷レポート · 研究参考用
Bromine → HCID 178516705、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Bromine | HCID 24408 | — |
| 反応物 | HCID 178516710 | HCID 178516710 | — |
| 溶媒 | Acetic Acid | HCID 176 | — |
| 生成物 | HCID 178516705 | HCID 178516705 | 90% |
反応手順
Bromine (0.895 mL, 15.5 mmol) was added to the solution of quinoxalin-2-ol (1.5 g, 10.3 mmol) in HOAc (15 mL), the mixture was stirred at r.t. for 6 h, and the precipitate was collected and washed with ethyl ether and dried to afford 7-bromoquinoxalin-2-ol as a solid in 90% yield (2 g).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09181264B2 |
| 出典データセット | uspto-grants-2015_11 |
| ORD ID | ord-f19a51d543424f9b8ea1bc10a8a907b6 |
| 出典メモ | uspto-grants-2015_11 |