関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Triphenylphosphine | HCID 11776 | — |
| 反応物 | 10-Bromodecanoic Acid | HCID 142712 | — |
| 生成物 | (9-Carboxynonyl)(triphenyl)phosphanium bromide | HCID 18795071 | 100% |
反応手順
10-Bromodecanoic acid (19.65 g, 78.24 mmol) and triphenylphosphine (21.45 g, 81.78 mmol) were mixed and stirred at 150° C. for 24 h. Wittig reagent B2 as light yellow syrup was obtained in 100% yield and used without further purification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US09181292B2 |
|---|
| 出典データセット | uspto-grants-2015_11 |
|---|
| ORD ID | ord-5b62cc87cd204da78be882dda48f884b |
|---|
| 出典メモ | uspto-grants-2015_11 |
|---|
