化工社化工社 化学情報印刷レポート · 研究参考用
2-Aminobiphenyl → N2,N4-bis(2-phenylphenyl)-5-methyl-2,4-pyrimidinediamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Aminobiphenyl | HCID 7015 | — |
| 反応物 | Pyrimidine, 2,4-dichloro-5-methyl- | HCID 74508 | — |
| 生成物 | N2,N4-bis(2-phenylphenyl)-5-methyl-2,4-pyrimidinediamine | HCID 22060710 | — |
反応手順
In like manner to the preparation of 5-fluoro-N2,N4-bis(3-hydroxyphenyl)-2,4-pyrimidinediamine, 2-aminobiphenyl and 2,4-dichloro-5-methylpyrimidine were reacted to provide N2,N4-bis(2-phenylphenyl)-5-methyl-2,4-pyrimidinediamine. LCMS: ret. time: 30.47 min.; purity: 91%; MS (m/e): 429 (MH+).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08822685B2 |
| 出典データセット | uspto-grants-2014_09 |
| ORD ID | ord-545dcb3821fb4a3cbfe6b60d9b96d913 |
| 出典メモ | uspto-grants-2014_09 |