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Benzoylhydrazine → N-(4-(2-(2-phenylacetyl)hydrazinecarbonyl)pyridin-2-yl)benzamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzoylhydrazine | HCID 11955 | — |
| 反応物 | Benzeneacetic acid, hydrazide | HCID 70301 | — |
| 反応物 | 2-Benzamidoisonicotinic acid | HCID 64393851 | — |
| 生成物 | N-(4-(2-(2-phenylacetyl)hydrazinecarbonyl)pyridin-2-yl)benzamide | HCID 67153966 | 65% |
反応手順
Following the procedure as described in Preparation 13, making variations as required to replace benzohydrazide with 2-phenylacetohydrazide to react with 2-benzamidoisonicotinic acid, N-(4-(2-(2-phenylacetyl)hydrazinecarbonyl)pyridin-2-yl)benzamide was obtained in 65% yield: MS (ES+) m/z 374.9 (M+1).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09187426B2 |
| 出典データセット | uspto-grants-2015_11 |
| ORD ID | ord-041b11ff412e435fbd512076e40afaa5 |
| 出典メモ | uspto-grants-2015_11 |