Methacrylic Acid → Solanone

HRID 716607ノート

反応式

HRID 716607 の反応式
C(O)(=O)C(C)=C.CC(C(OCCOC(C(C)=C)=O)=O)=C.[CH:21]([CH:24]([CH2:30][CH2:31][CH:32]([CH3:34])[CH3:33])[CH2:25][CH2:26][C:27](=[O:29])[CH3:28])([CH3:23])[CH3:22]>C1(C)C=CC=CC=1>[CH3:23][CH:21]([C@@H:24](/[CH:30]=[CH:31]/[C:32]([CH3:34])=[CH2:33])[CH2:25][CH2:26][C:27]([CH3:28])=[O:29])[CH3:22]

参加物

5

反応物 3

HCID 4093Methacrylic AcidHCID 7355Ethylene glycol dimethacrylateHCID 89183541HCID 89183541、化合物

生成物 1

HCID 6451337Solanone

試薬・触媒・溶媒 1

HCID 1140Toluene溶媒

実験手順

Methacrylic acid (3 mol percent), EGDMA (95 mol percent), and 5-isopropyl-8-methylnonan-2-one (2 mol percent) are combined in toluene. 2,2-Azobisisobutyronitrile (AIBN) is added as an initiator. The reaction flask is degassed, purged with dry nitrogen, and sealed. The solution is irradiated with a UV lamp (365 nm) to activate the AIBN and initiate the polymerization reaction.

後処理

  1. customThe reaction flask is degassed
  2. custompurged with dry nitrogen
  3. customsealed
  4. customThe solution is irradiated with a UV lamp (365 nm)
  5. customthe polymerization reaction

出典と根拠

ORDレコード
ord-b5ac5cf49dcf4455a1dc12b61b82caa9
出典データセット
uspto-grants-2015_11
特許番号
US09192193B2

反応ノート

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