Selenium Dioxide → HCID 12336408、化合物
反応式
[Cl:1][C:2]1[CH:11]=[CH:10][CH:9]=[C:8]2[C:3]=1[CH2:4][CH2:5][CH2:6][C:7]2=[O:12].[Se](=O)=[O:14]>>[Cl:1][C:2]1[CH:11]=[CH:10][CH:9]=[C:8]2[C:3]=1[CH:4]=[CH:5][C:6](=[O:14])[C:7]2=[O:12]参加物
3
実験手順
Treatment of 5-chloro-tetralone with selenium dioxide as described in Reference Example 1A yielded 5-chloro-[1,2]naphthoquinone which was coupled with 2,3-diamino-benzoic acid, diacetate salt, as described in Reference Example 1A to yield the title compound.
出典と根拠
- ORDレコード
- ord-d106eb56aafe48c58c86d8d7b177349d
- 出典データセット
- uspto-grants-2006_11
- 特許番号
- US07132419B2
反応ノート
読み込み中…