Selenium Dioxide → 5-Ethoxy-[1,2]naphthoquinone
反応式
[CH2:1]([O:3][C:4]1[CH:13]=[CH:12][CH:11]=[C:10]2[C:5]=1[CH2:6][CH2:7][CH2:8][C:9]2=[O:14])[CH3:2].[Se](=O)=[O:16]>>[CH2:1]([O:3][C:4]1[CH:13]=[CH:12][CH:11]=[C:10]2[C:5]=1[CH:6]=[CH:7][C:8](=[O:16])[C:9]2=[O:14])[CH3:2]参加物
3
実験手順
Treatment of 5-ethoxy-1-tetralone with selenium dioxide as described in Reference Example 1A yielded 5-ethoxy-[1,2]naphthoquinone which was coupled with 2,3-diamino-benzoic acid, diacetate salt, as described to yield the title compound.
出典と根拠
- ORDレコード
- ord-2950a6629865481ab5482681b38ced5a
- 出典データセット
- uspto-grants-2006_11
- 特許番号
- US07132419B2
反応ノート
読み込み中…