化工社化工社 化学情報印刷レポート · 研究参考用
2-Amino-4-(4-methoxyphenyl)thiazole → 2,4,6-trichloro-N-[4-(4-methoxyphenyl)-1,3-thiazol-2-yl]benzenesulfonamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Amino-4-(4-methoxyphenyl)thiazole | HCID 159644 | — |
| 反応物 | 2,4,6-Trichlorobenzenesulfonyl chloride | HCID 521335 | — |
| 生成物 | 2,4,6-trichloro-N-[4-(4-methoxyphenyl)-1,3-thiazol-2-yl]benzenesulfonamide | HCID 10114786 | — |
反応手順
The title compound was prepared from 4-(4-methoxy-phenyl)-thiazol-2-ylamine and 2,4,6-trichlorobenzenesulfonyl chloride as described in the synthetic MEIHOD B to give a white-yellow solid (58.2 mg) with purity >90%. MS (pos) m/z 449.1, 451.1, 453.1.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07132436B2 |
| 出典データセット | uspto-grants-2006_11 |
| ORD ID | ord-0af05847f737479084086a2f83fd0da0 |
| 出典メモ | uspto-grants-2006_11 |