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4-(3-Pyridinyl)-2-thiazolamine → 2,4,6-Trichloro-N-[4-(3-pyridinyl)-1,3-thiazol-2-yl]benzenesulfonamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-(3-Pyridinyl)-2-thiazolamine | HCID 154893 | — |
| 反応物 | 2,4,6-Trichlorobenzenesulfonyl chloride | HCID 521335 | — |
| 生成物 | 2,4,6-Trichloro-N-[4-(3-pyridinyl)-1,3-thiazol-2-yl]benzenesulfonamide | HCID 10136952 | — |
反応手順
The title compound was prepared from 4-(3-pyridyl)-1,3-thiazol-2-amine and 2,4,6-trichlorobenzenesulfonyl chloride as described in the synthetic METHOD B to give a yellow solid (29.3 mg) with purity >90%: MS (pos) m/z 422.1; HRMS m/z 418.9134 (calc. of monoisotopic mass for C14H8Cl3N3O2S2 gives 418.9123).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07132436B2 |
| 出典データセット | uspto-grants-2006_11 |
| ORD ID | ord-f6ee2e41f3e4460f9237787acfbcc012 |
| 出典メモ | uspto-grants-2006_11 |