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3-Chloro-2-methylbenzenesulfonyl chloride → 3-Chloro-N-[4-(3-chloro-2-thienyl)-1,3-thiazol-2-yl]-2-methylbenzenesulfonamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-Chloro-2-methylbenzenesulfonyl chloride | HCID 522734 | — |
| 反応物 | 4-(3-Chloro-2-thienyl)-1,3-thiazol-2-amine | HCID 1488441 | — |
| 生成物 | 3-Chloro-N-[4-(3-chloro-2-thienyl)-1,3-thiazol-2-yl]-2-methylbenzenesulfonamide | HCID 10135902 | — |
反応手順
The title compound was prepared from 4-(3-chloro-2-thienyl)-1,3-thiazol-2-amine and 3-chloro-2-methylbenzenesulfonyl chloride as described in the synthetic METHOD B to give a white-yellow solid (7.6 mg) with purity >90%. MS (pos) m/z 405.2, 407.2.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07132436B2 |
| 出典データセット | uspto-grants-2006_11 |
| ORD ID | ord-e85357db423e44d99ecdbbda00db20af |
| 出典メモ | uspto-grants-2006_11 |